Analysis of Intermediate Propiophenone used in Pharmaceutical Industry by Gas Chromatography and Mass Spectrometry; 实验研究了以氯化苄为原料合成药物中间体苯基丙酮的新工艺。
A new method for the determination of propiophenone content by gas chromatography and mass spectrometry ( GC-MS) was established. 本文建立了用气相色谱/质谱法(GC/MS)测定苯丙酮含量的方法。
Hydroxy 2 methyl 1 propiophenone was synthesized in four steps with benzaldehyde, 2 bromopropane and bromine as main raw materials. 以苯甲醛、镁、2-溴丙烷、溴等为主要原料,经四步反应合成了光敏引发剂2-羟基-2-甲基-1-苯基丙酮。
Objective: To set up a new method for the determination of phenylpropanol and propiophenone in phenylpropanol soft capsules by GC-MS. 目的:建立了GC-MS法测定苯丙醇胶丸中苯丙醇含量及其杂质苯丙酮的含量。